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Also, the inefficient removal of TMA may result in the development of 'fishy odor' syndrome

Example-20: Preparation of Semaglutide side chain (compound of formula-3a) Step 1: Preparation of compound of formula-9 DIPEA (11.3 ml) and TSTU (19.52 gm) were added to a mixture of compound of formula-8 (30 gm) and acetonitrile (180 ml) at 25-30C and stirred the mixture for 2 hr at the same temperature

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