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Coupling of Fmoc-Lys(biotin)-OH : To a solution of HATU (190 mg, 0.500 mmol, 5 equiv) in DMF (3 mL) were successively added Fmoc-Lys(biotin)-OH (300 mg, 0.504 mmol, 5 equiv) and DIEA (173 L, 1.00 mmol, 10 equiv) and the mixture was stirred at rt for 2 min